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Synthesis and Characterization of Zinc (II) Complexes with 3, 4-Dimethoxybenzaldehyde Thiosemicarbazone: The Crystal Structure of [Zn (34-MBTSC) 2Cl2]

…, G Grivani, M Rezaei, K Fejfarova…

文献索引:Khalaji, Aliakbar Dehno; Grivani, Gholamhossein; Rezaei, Morteza; Fejfarova, Karla; Dusek, Michal Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 8 p. 1119 - 1126

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被引用次数: 2

摘要

The synthesis and characterization of three zinc(II) complexes [Zn(34-MBTSC) 2 Cl 2 ] (1), [Zn(34-MBTSC) 2 Br 2 ] (2), and [Zn(34-MBTSC) 2 I 2 ] (3) of 3,4-dimethoxybenzaldehyde thiosemicarbazone (34-MBTSC) are reported. Elemental analysis (CHN) and spectral (FT-IR and 1 H-NMR) measurements have been used to characterize the complexes. In addition, the structure of the complex 1 has been determined by X-ray diffraction methods. In these complexes, the zinc(II) ion is ...