Synthesis and the Crystal Structure of (E)-2-(7-(3-(Thiophen-2-yl) acrylamido)-2, 3-dihydro-5-oxobenzo [e][1, 4] oxazepin-1 (5H)-yl) ethyl acetate

YJ Lee, JR King, BC Chenna, SB Owens Jr…

文献索引：Lee, Yun J.; King, Jason R.; Chenna, Bala Chandra; Owens Jr., Samuel B.; Freeman, Jason L.; Gray, Gary M.; Velu, Sadanandan E. Journal of Chemical Crystallography, 2009 , vol. 39, # 12 p. 902 - 907

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摘要

Abstract Details of the synthesis and crystal structure determination of (E)-2-(7-(3-(thiophen- 2-yl) acrylamido)-2, 3-dihydro-5-oxobenzo [e][1, 4] oxazepin-1 (5H)-yl) ethyl acetate are presented. The compound crystallizes in the triclinic P− 1 space group (a= 8.3377 (17), b= 9.792 (2), c= 12.469 (3) Å, α= 96.39 (3)°, β= 108.50 (3)°, γ= 97.68 (3)°, V= 943.9 (3) Å 3, Z= 2). Interesting features of the structure include intermolecular hydrogen bonding between ...