... George R. Newkome,* Charles N. Moorefield, and Kevin J. Theriot Department of Chemistry, University of South ... The combined organic extract was concentrated to give (95%) the pure nitro triol: 800 mg ... CHzCHzOH, 6 H), 1.92 (m, CH2CHzCH20H, 6 H), 3.39 (t, CH,OH, J = 6.0 Hz ...