A highly convergent synthesis of benzimidazolylpiperidines

…, DA Hay, JM Kane, MA Staeger

文献索引：Carr, Albert A.; Hay, David A.; Kane, John M.; Staeger, Michael A. Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1399 - 1401

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被引用次数: 5

摘要

Chloroacetic acid in the ozonolysis of (li) was identified by comparing the mass spectrum with that of authentic sample and determined by gas chromatography. The conditions were as follows: column, 2% FFAP on Gas Chrom Q (80-100 mesh), 4 mm X 1 m, glass; column temperature, 80-210" C, programmed at 10 OC min-'; injection temperature, 220" C; detector temperature, 240 OC; detector, FID.