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Consistency of NMR and mass spectrometry determinations of natural-abundance site-specific carbon isotope ratios. The case of glycerol

BL Zhang, M Trierweiler, C Jouitteau…

文献索引:Zhang; Trierweiler; Jouitteau; Martin Analytical Chemistry, 1999 , vol. 71, # 13 p. 2301 - 2306

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被引用次数: 20

摘要

Quantitative determinations of natural-abundance carbon isotope ratios by nuclear magnetic resonance (SNIF-NMR) have been optimized by appropriate selection of the experimental conditions and by signal analysis based on a dedicated algorithm. To check the consistency of the isotopic values obtained by NMR and mass spectrometry (IRMS) the same glycerol samples have been investigated by both techniques. To have access to site-specific ...