Reactions of β-alkoxyvinyl trifluoromethyl ketones. The synthesis of N-[1-aryl-3-oxo-4, 4, 4-trifluoro-1-buten-1-yl]-o-phenylenediamines and 4-aryl-2-trifluoromethyl-3H- …

…, L Magali Leão Marques, N Zanatta…

文献索引：Gauze Bonacorso, Helio; Leao Marques, Livete Magali; Zanatta, Nilo; Pinto Martins, Marcos Antonio Synthetic Communications, 2002 , vol. 32, # 20 p. 3225 - 3232

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被引用次数: 27

摘要

ABSTRACT A series of five N-[1-aryl-3-oxo-4, 4, 4-trifluoro-1-buten-1-yl]-o- phenylenediamines 2 [CF3COCH= C (R) NH-o-PhNH2], where R= Ph, 4-MePh, 4-BrPh, 4- ClPh, 4-OMePh from the reaction of β-aryl-β-methoxyvinyl trifluoromethyl ketones 1 with o- phenylenediamine was prepared and isolated in good yield (59–71%). Another series of five 4-aryl-2-trifluoromethyl-3H-1, 5-benzodiazepines 3, where aryl= Ph, 4-MePh, 4-BrPh, 4- ...