The Journal of organic chemistry

Silicon carbide passive heating elements in microwave-assisted organic synthesis

JM Kremsner, CO Kappe

文献索引：Kremsner, Jennifer M.; Kappe, C. Oliver Journal of Organic Chemistry, 2006 , vol. 71, # 12 p. 4651 - 4658

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被引用次数: 160

摘要

Microwave-assisted organic synthesis in nonpolar solvents is investigated utilizing cylinders of sintered silicon carbide (SiC) a chemically inert and strongly microwave absorbing material as passive heating elements (PHEs). These heating inserts absorb microwave energy and subsequently transfer the generated thermal energy via conduction phenomena to the reaction mixture. The use of passive heating elements allows otherwise microwave ...