Two redox methods are descrlbed for the determlnation of carboxylic acid anhydrides involving reactlon with elther an excess of 4-amlnophenol or a measured but excessive amount of sulfanllamlde and photometrlc tltratlon of N-acyl-4-amlnophenol with 2- iodylbenroate by measurlng the absorbance of orange-red product at 444 nm or the residual amount of sulfanilamide Is determlned by tltratlon with chloramine-T In the presence of ...