... Compound 18b (M = Pd) was characterized by single-crystal X-ray analysis ... This procedure was modeled after that reported by Bouda et al ... 13 The reaction proceeds smoothly over 12 h at ambient temperature, and the product can be isolated by vacuum transfer from the reaction ...
[Kleiner, Christian M.; Horst, Luise; Wuertele, Christian; Wende, Raffael; Schreiner, Peter R. Organic and Biomolecular Chemistry, 2009 , vol. 7, # 7 p. 1397 - 1403]