Decarbonylative Radical Cyclization of α-Amino Selenoesters upon Electrophilic Alkenes. A General Method for the 6-Azabicyclo [3.2. 1] octane Synthesis

J Quirante, X Vila, C Escolano…

文献索引：Mellor, John M.; Pathirana, Ranjith; Stibbard, John H.A. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2541 - 2544

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被引用次数: 44

摘要

... The Journal of Organic ... phase was extracted with CH 2 Cl 2 . Concentration of the dried organic extracts gave a residue, which was purified by chromatography (CH 2 Cl 2 ), to yield diester 8 as an orange oil (678 mg, 85%): IR (NaCl) 1717; 1 H NMR 1.40−1.60 (m, 1H), 1.45 ...