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Organometallics

Crystal structures of (. mu.-trithio) bis [tricyclohexylgermanium (IV)] and (. mu.-trithio) bis [triphenylgermanium (IV)]

…, M Vanier, MJ Olivier, Y Gareau, K Steliou

文献索引:Brisse, Francois; Vanier, Micheline; Olivier, Marc J.; Gareau, Yves; Steliou, Kosta Organometallics, 1983 , vol. 2, p. 878 - 882

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被引用次数: 8

摘要

= 394, Cu Ka radiation, p (Cu Ka)= 3.59 mm-I. The structure, solved by direct methods, was refined by least squares to a final R value of 0.063 for 3185 observed reflections.[(CsH5) 3Ge] 2S3 (11),(p-trithio)-bis [triphenylgermanium (IV)], is monoclinic of space group P2,/n. The unit cell has the following dimensions: a= 11.969 (5) A, b= 17.982 (6) A, c= 16.741 (9) A, p= 100.37 (4) O, V= 3543.9 A3, dcdcd= 1.319 Mg m-,, 2= 4, F (000)= 1432, Mo Ka ...