The Preparation and Reaction of Some Substituted Benzotrifluorides

TC Frazier, CR WALTER Jr…

文献索引：Frazier,T.C. et al. Journal of Organic Chemistry, 1961 , vol. 26, p. 2223 - 2225

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被引用次数: 3

摘要

4-Etho22/-6-nitrobenzotriJEuoride (11). A solution of 22.5 g.(0.10 mole) of 4-chloro-3- nitrobenzotrifluoride (I) in absolute ethanol (60 cc. total volume) was added during 1 hr. t'o a solution of 300 cc. of absolute ethanol containing 5.6 g. of potassium hydroxide. After refluxing 72 hr. the ethanol vas removed at reduced pressure, arid inorganic sa. lts were removed by slurrying the residue with ethyl ether and filtering. An oily-crystalline slurry ...