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举例 :可输入Filippa Pettersson 或者 Cancer Res. 75(6) , 1102-12, (2015) 或者10.1002/anie.201600521

[2+ 2+ 2]??Cycloaddition of 4??Hydroxy??Substituted Enediynes to 2??Hydroxy??Substituted Decahydrophenanthrenes

U Groth, N Richter, A Kalogerakis

文献索引：Groth, Ulrich; Richter, Norbert; Kalogerakis, Aris European Journal of Organic Chemistry, 2003 , # 23 p. 4634 - 4639

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被引用次数: 10

摘要

Abstract Enediynes rac-4 were prepared in seven steps with an overall yield of 31% starting from 4-pentyn-1-ol (5). A cobalt mediated [2+ 2+ 2]-cycloaddition of these enediynes and subsequent removal of the metal fragment afforded the decahydrophenanthrenes rac-3/13 in 37− 56% yield.(© Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2003)

(E)-1-(tert-butyldimethylsilyloxy)-4-methyl-11-(trimethylsilyl)-undec-4-en-10-yne结构式

(E)-1-(tert-but...

~82%

4-methylundec-4-en-10-yn-1-ol结构式

4-methylundec-4...

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4-戊炔-1-醇结构式

~%

4-methylundec-4-en-10-yn-1-ol结构式

4-methylundec-4...

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5-己炔-1-醇结构式

~%

4-methylundec-4-en-10-yn-1-ol结构式

4-methylundec-4...

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6-(三甲基甲硅烷基)己-5-炔-1-醇结构式

6-(三甲基甲硅烷基)己-5-炔-1-醇

~%

4-methylundec-4-en-10-yn-1-ol结构式

4-methylundec-4...

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6-(trimethylsilyl)-5-hexynyl methanesulfonate结构式

6-(trimethylsil...

~%

4-methylundec-4-en-10-yn-1-ol结构式

4-methylundec-4...

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6-bromohex-1-ynyl(trimethyl)silane结构式

6-bromohex-1-yn...

~%

4-methylundec-4-en-10-yn-1-ol结构式

4-methylundec-4...

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(E)-1-iodo-2-methyl-1-penten-5-ol结构式

(E)-1-iodo-2-me...

~%

4-methylundec-4-en-10-yn-1-ol结构式

4-methylundec-4...

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未登录结构式

~%

4-methylundec-4-en-10-yn-1-ol结构式

4-methylundec-4...

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4-methylundec-4-en-10-yn-1-ol结构式

4-methylundec-4...

~77%

4-methylundec-4-en-10-ynal结构式

4-methylundec-4...

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4-戊炔-1-醇结构式

~%

4-methylundec-4-en-10-ynal结构式

4-methylundec-4...

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5-己炔-1-醇结构式

~%

4-methylundec-4-en-10-ynal结构式

4-methylundec-4...

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6-(三甲基甲硅烷基)己-5-炔-1-醇结构式

6-(三甲基甲硅烷基)己-5-炔-1-醇

~%

4-methylundec-4-en-10-ynal结构式

4-methylundec-4...

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6-(trimethylsilyl)-5-hexynyl methanesulfonate结构式

6-(trimethylsil...

~%

4-methylundec-4-en-10-ynal结构式

4-methylundec-4...

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6-bromohex-1-ynyl(trimethyl)silane结构式

6-bromohex-1-yn...

~%

4-methylundec-4-en-10-ynal结构式

4-methylundec-4...

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(E)-1-iodo-2-methyl-1-penten-5-ol结构式

(E)-1-iodo-2-me...

~%

4-methylundec-4-en-10-ynal结构式

4-methylundec-4...

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未登录结构式

~%

4-methylundec-4-en-10-ynal结构式

4-methylundec-4...

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(E)-1-(tert-butyldimethylsilyloxy)-4-methyl-11-(trimethylsilyl)-undec-4-en-10-yne结构式

(E)-1-(tert-but...

~%

4-methylundec-4-en-10-ynal结构式

4-methylundec-4...

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溴代丙炔结构式

4-methylundec-4-en-10-ynal结构式

4-methylundec-4...

~73%

7-methyltetradec-7-en-1,13-diyn-4-ol结构式

7-methyltetrade...

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4-戊炔-1-醇结构式

~%

7-methyltetradec-7-en-1,13-diyn-4-ol结构式

7-methyltetrade...

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5-己炔-1-醇结构式

~%

7-methyltetradec-7-en-1,13-diyn-4-ol结构式

7-methyltetrade...

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6-(三甲基甲硅烷基)己-5-炔-1-醇结构式

6-(三甲基甲硅烷基)己-5-炔-1-醇

~%

7-methyltetradec-7-en-1,13-diyn-4-ol结构式

7-methyltetrade...

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6-(trimethylsilyl)-5-hexynyl methanesulfonate结构式

6-(trimethylsil...

~%

7-methyltetradec-7-en-1,13-diyn-4-ol结构式

7-methyltetrade...

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6-bromohex-1-ynyl(trimethyl)silane结构式

6-bromohex-1-yn...

~%

7-methyltetradec-7-en-1,13-diyn-4-ol结构式

7-methyltetrade...

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(E)-1-iodo-2-methyl-1-penten-5-ol结构式

(E)-1-iodo-2-me...

~%

7-methyltetradec-7-en-1,13-diyn-4-ol结构式

7-methyltetrade...

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未登录结构式

~%

7-methyltetradec-7-en-1,13-diyn-4-ol结构式

7-methyltetrade...

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4-methylundec-4-en-10-yn-1-ol结构式

4-methylundec-4...

~%

7-methyltetradec-7-en-1,13-diyn-4-ol结构式

7-methyltetrade...

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(E)-1-(tert-butyldimethylsilyloxy)-4-methyl-11-(trimethylsilyl)-undec-4-en-10-yne结构式

(E)-1-(tert-but...

~%

7-methyltetradec-7-en-1,13-diyn-4-ol结构式

7-methyltetrade...

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7-methyltetradec-7-en-1,13-diyn-4-ol结构式

7-methyltetrade...

碘甲烷结构式

~82%

4-methoxy-7-methyltetradec-7-en-1,13-diyne结构式

4-methoxy-7-met...

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4-戊炔-1-醇结构式

~%

4-methoxy-7-methyltetradec-7-en-1,13-diyne结构式

4-methoxy-7-met...

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(E)-1-iodo-2-methyl-1-penten-5-ol结构式

(E)-1-iodo-2-me...

~%

4-methoxy-7-methyltetradec-7-en-1,13-diyne结构式

4-methoxy-7-met...

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未登录结构式

~%

4-methoxy-7-methyltetradec-7-en-1,13-diyne结构式

4-methoxy-7-met...

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4-methylundec-4-en-10-ynal结构式

4-methylundec-4...

~%

4-methoxy-7-methyltetradec-7-en-1,13-diyne结构式

4-methoxy-7-met...

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4-methylundec-4-en-10-yn-1-ol结构式

4-methylundec-4...

~%

4-methoxy-7-methyltetradec-7-en-1,13-diyne结构式

4-methoxy-7-met...

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(E)-1-(tert-butyldimethylsilyloxy)-4-methyl-11-(trimethylsilyl)-undec-4-en-10-yne结构式

(E)-1-(tert-but...

~%

4-methoxy-7-methyltetradec-7-en-1,13-diyne结构式

4-methoxy-7-met...

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6-(trimethylsilyl)-5-hexynyl methanesulfonate结构式

6-(trimethylsil...

~86%

6-bromohex-1-ynyl(trimethyl)silane结构式

6-bromohex-1-yn...

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5-己炔-1-醇结构式

~%

6-bromohex-1-ynyl(trimethyl)silane结构式

6-bromohex-1-yn...

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