Synthesis of functionalized bicyclo [3.2. 1] octa-2, 6-dienes by thermal rearrangement of substituted 6-exo-(1-alkenyl) bicyclo [3.1. 0] hex-2-ene systems
E Piers, GL Jung, EH Ruediger
文献索引:McErlean, Christopher S. P.; Proisy, Nicolas; Davis, Christopher J.; Boland, Nicola A.; Sharp, Swee Y.; Boxall, Kathy; Slawin, Alexandra M. Z.; Workman, Paul; Moody, Christopher J. Organic and Biomolecular Chemistry, 2007 , vol. 5, # 3 p. 531 - 546
... The others, 15-17, were prepared via relatively straightforward chemistry. ... The organic phase was washed with 5% hydro- chloric acid, brine, and saturated aqueous sodium bicarbonate and then was dried ... oil; ir (film): 3300, 1660 cm-I; 'H nmr (80 MHz), 6: 1.00 (d, 6H, J = 7 Hz ...