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Journal of Chemical and Engineering Data

Preparation of sterically hindered phosphoramidates

JJ Talley

文献索引:Talley, John J. Journal of Chemical & Engineering Data, 1988 , vol. 33, # 2 p. 221 - 222

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被引用次数: 15

摘要

Treatment of phosphorus oxychloride with two equivalents of 2, 64methyIphend In the presence of magnedum chloride produced the sterlcally hlndered bls (2, 8dhnethylphenyl) chlorophosphate In excellent yield. The dlaryl phosphorochlorldete reacted with a variety of primary and secondary amines to produce phosphoramldates In good to excellent yield.