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Journal of the American Chemical Society

8-Nitro-7-methoxyisoquinoline

M Kulka

文献索引:Kulka Journal of the American Chemical Society, 1953 , vol. 75, p. 3597

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被引用次数: 6

摘要

Experimental 7-Methoxy-8-nitroisoquinoline.-To a stirred solution of 7-methoxyi~ oquinoline~(7.0 8.) in concentrated sulfuric acid (100 cc.) was added portionwise a solution of potassium nitrate (5.0 g.) in concentrated sulfuric acid (35 cc.) while the temperature was maintained at 0-5" by cooling. After stirring for an additional one-half hour at G5", the reaction mixture was poured onto cracked ice. The resulting solution was basified and the ...