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Journal of the American Chemical Society

THE ORIENTATION OF THE BROMINE ATOM IN BROMODIMETHOXYBENZOIC ACID

GP Rice

文献索引:Rice Journal of the American Chemical Society, 1926 , vol. 48, p. 3127

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被引用次数: 8

摘要

5-Bromo-2, 4-dimethoxybenzoic Acid,(CH30) 2CsHzBrCOOH.-The acid obtained in quantitative yield by the oxidation of 5-bromo-2, 4-dimethoxybenzoylacrylic acid with potassium permanganate can be purified by recrystallization from acetone or xylene. It melts at 193" and is sparingly soluble in boiling water, acetone, xylene, chloroform and methyl alcohol.