Tetrahedron Letters

A modified Curtius reaction: an efficient and simple method for direct isolation of free amine

B Ma, WC Lee

文献索引：Tetrahedron Letters, , vol. 51, # 2 p. 385 - 386

全文：HTML全文

被引用次数: 17

摘要

... Tetrahedron Letters. ... 8. In this Letter, we now report a very simple modification of Curtius reaction by quenching the isocyanate intermediates (3) with sodium trimethylsilanolate (NaOTMS), which provides an efficient one-pot method for direct isolation of ... Tetrahedron, 60 (2004), pp ...