Synthetic communications

A new preparation of gem-bis (difluoramino)-alkanes via direct fluorination of geminal bisacetamides

RD Chapman, MC Davis, R Gilardi

文献索引：Chapman, Robert D.; Davis, Matthew C.; Gilardi, Richard Synthetic Communications, 2003 , vol. 33, # 23 p. 4173 - 4184

全文：HTML全文

被引用次数: 6

摘要

Abstract A fundamentally new preparation of internal and terminal gem-bis-(difluoramino) alkanes has been demonstrated by the direct fluorination of corresponding gem- bisacetamides, specifically, 1, 1-bisacetamidocyclohexane and 1, 1-bisacetamidopropane, leading to 1, 1-bis (difluoramino) cyclohexane and 1, 1-bis (difluoramino)-propane, respectively.