An efficient H 2 NSO 3 H??catalyzed protection of various carbonyl compounds at room temperature was investigated. The features of mild conditions, cost??efficient catalyst, simple workup, and the recyclability of the catalyst were represented in this process. ... An efficient H 2 NSO 3 H??catalyzed protection of various carbonyl compounds at room temperature was investigated. The features of mild conditions, cost??efficient catalyst, simple workup, and ...