Syntheses based on nitrile oxides

…, YA Strelenko, NV Obruchnikova, LI Khmel'nitskii

文献索引：Ogurtsov, V. A.; Rakitin, O. A.; Strelenko, Yu. A.; Obruchnikova, N. V.; Khmel'nitskii, L. I. Russian Chemical Bulletin, 1993 , vol. 42, # 4 p. 706 - 708 Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 4 p. 742 - 743

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摘要

GLC-analysis was carried out with a Biokhrom IM chromatograph on a glass column (58.5x0.25 mm) with a PEG-40M stationary liquid phase and nitrogen as the carrier gas. NMR spectra were recorded with a Bruker AM-300 spectrometer at working frequencies of 300 MHz for IH, 75.5 MHz for 13C, 21.7 MHz for 14N, and 30.4 MHz for 15N. The reactions of t-BuNHMgBr and t-BuNHLi with nitro com- pounds were carded out according to the previously ...