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Journal of the American Chemical Society

p-AMINOBENZONITRILE AND CERTAIN OF ITS DERIVATIVES.[THIRD PAPER.] 1

MT Bogert, LE Wise

文献索引:Bogert; Wise Journal of the American Chemical Society, 1912 , vol. 34, p. 701

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被引用次数: 5

摘要

fi-Aminobenzonitrile was prepared as described in our previous paper, the nitrile being purified by crystallization from water. Instead of attempting to recover the nitrile in the mother liquors by concentration, it was found much more convenient to heat these aqueous mother liquors direct with excess of acetic anhydride, the nitrile being then thrown out in a few minutes as the crystallin acetyl derivative. Picrate.-I. 8 grams of picric acid were dissolved ...