Synthetic communications

Mild Microwave??Assisted Hydrolysis of Acetals Under Solvent??Free Conditions

Y He, M Johansson, O Sterner

文献索引：He, Yanhong; Johansson, Martin; Sterner, Olov Synthetic Communications, 2004 , vol. 34, # 22 p. 4153 - 4158

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被引用次数: 12

摘要

Abstract Acetals are efficiently hydrolyzed with silica gel??supported pyridinium tosylate moistened with water in solvent??free conditions under microwave irradiation. The method is efficient and mild, with acid??sensitive 3??hydroxyacetals and 3??methoxyacetals being hydrolyzed in minutes in good yields.