The Journal of Organic Chemistry

Preparation of solid thianthrene cation radical tetrafluoroborate

B Boduszek, HJ Shine

文献索引：Journal of Organic Chemistry, , vol. 53, # 21 p. 5142 - 5143

被引用次数: 53

摘要

... (1) On leave from the Institute of Organic and Physical Chemistry, (2) Murata ... purified by reprecipitating from methylene chloride with ether, giving 5-methylthianthreniumyl tetrafluoroborate (eq 2, R = Me): mp 194-196 "C dec; 'H NMR (CDC13CD3CN) 6 8.22 (d, 2 H, J = 7.6 Hz ...

~91%

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