Tetrahedron

Optimisation and scale-up of microwave assisted cyanation

MR Pitts, P McCormack, J Whittall

文献索引：Tetrahedron, , vol. 62, # 19 p. 4705 - 4708

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被引用次数: 52

摘要

... Tetrahedron. Volume 62, Issue 19, 8 May 2006, Pages 4705–4708. ... 2) the bromo starting material 1 (56.0 g, 148 mmol), zinc cyanide (ground to 600 micron powder, 10.8 g, 92 mmol, 0.62 equiv) and TMEDA (4.8 mL, 32 mmol, 0.22 equiv) slurried in DMF to a total volume of 160 ...