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Improved Process for the Preparation of 6-Chloro-5-(2-chloroethyl) oxindole

DV Nadkarni, JF Hallissey

文献索引:Organic Process Research and Development, , vol. 12, # 6 p. 1142 - 1145

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被引用次数: 20

摘要

... The organic layer was concentrated to a volume of 10−15 L by distillation under reduced pressure ... and supply chain analytical control department who contributed to the successful scale-up of this process. ... 1 H and 13 C NMR for compounds 1, 5, and 6; general procedure for the ...