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The syntheses of mono-and disubstituted phthalocyanines using a dithioimide

…, S Greenberg, B Khouw, ABP Lever

文献索引:Leznoff, Clifford C.; Greenberg, Shafrira; Khouw, Ben; Lever, A. B. P. Canadian Journal of Chemistry, 1987 ,  vol. 65, p. 1705 - 1713

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被引用次数: 46

摘要

Hydrolysis of 5-neopentoxy-1, 3-diiminoisoindoline gave 5-neopentoxy-1 H-isoindole-1, 3 (2 H)-dione (4-neopentoxyphthalimide), which, on treatment with Lawesson's reagent, yielded the thiophthalimides, 5-neopentoxy-1 H-isoindole-1, 3 (2 H)-dithione, 2, 3-dihydro-6- neopentoxy-3-thioxo-1 H-isoindol-1-one, and 2, 3-dihydro-5-neopentoxy-3-thioxo-1 H- isoindol-1-one. Attempted S-alkylations of the thiophthalimides resulted in the formation of ...