Journal of the American Chemical Society

Preparation of Nitro Compounds from Oximes. II. The Improved Synthesis of Nitrocycloalkanes1

DC Iffland, GX Criner

文献索引：Iffland; Criner Journal of the American Chemical Society, 1953 ,  vol. 75, p. 4047            

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被引用次数: 43

摘要

... a Ratio NBS to oxime was 2.5: 1. When NBS to oxime ratio is 1.1 : 1 yield is 22%; with ratio of 2: 1, yield is 58%. (1) Presented in part before the Division of Organic Chemistry of the American Chemical Society, Atlantic City, NJ, September 17, (2) DC Iffland, GX Criner, FJ Lotspeich, M. Koral, 2. B. (8) 0. Piloty and H. Steinbock, Be?., 81, 452 (1898). (4) C. Djerassi, Chrm. ... 2. Reaction temperature was 0-5'. (5) E. P. Kohler, THIS JOURNAL, 88, 887 (1916). ...