The Journal of Organic Chemistry

Synthesis of tert-butoxymethyl ethers: a new protecting group for alcohols

HW Pinnick, NH Lajis

文献索引：Pinnick,H.W.; Lajis,N.H. Journal of Organic Chemistry, 1978 , vol. 43, p. 3964 - 3966

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被引用次数: 14

摘要

We attempted to characterize enetriolate 1 by both UV-visible spectroscopy and 13C NMR spectroscopy. In the UV-visible spectrum 1 exhibits only end absorption even in dilute solution (ca. 1 XM). Absorption by other species in the base solution precluded measurement of either A,,, or an extinction coefficient. Solubility problems frustrated our at- tempts to measure the 13C NMR spectrum of 1. We have qualitatively measured the ...