Synthesis, spectroscopic characterization, mass spectrometry, and crystal structure of N-{[(4-bromophenyl) amino] carbonothioyl} benzamide

…, N Rashid, M BHATTI, P JONES

文献索引：Saeed, Sohail; Rashid, Naghmana; Bhatti, Moazzam Hussain; Jones, Peter G. Turkish Journal of Chemistry, 2010 , vol. 34, # 5 p. 761 - 770

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被引用次数: 8

摘要

Abstract: N-{[(4-bromophenyl) amino] carbonothioyl} benzamide was synthesized and characterized by IR,^ 1H-and^{13} C-NMR, mass spectrometry, and elemental analysis. The crystal structure was determined from single crystal X-ray diffraction data. It crystallizes in monoclinic space group P2_1/n with unit cell dimensions a= 13.822 (3) Å, b= 5.927 (2) Å, c= 16.642 (3) Å, and\ beta= 103.963 (3). There is a strong intramolecular hydrogen bond of ...