The Journal of Organic Chemistry

Synthesis and rearrangements of dihydro-1, 4-oxazepine and dihydro-1, 4-thiazepine derivatives

AP Krapcho, KJ Shaw

文献索引：Krapcho, A. Paul; Shaw, Kenneth J. Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3341 - 3343

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被引用次数: 8

摘要

L ation of their antitumor activity. l Our efforts in this research have uncovered some interesting heterocylic chemistry which we report. It had previously been reported by Cheng and coworkers1 that treatment of 1-chloroanthraquinone (lc) with the potassium salt of 2- (dimethy1amino) ethanol yielded Id (60%, isolated as the hydrochloride salt). Our initial attempt to prepare la was to react IC with 1 equiv of the sodium salt of 2-aminoethanol in ...