A convenient and stable synthon for ethyl azide and its evaluation in a [3+ 2]-cycloaddition reaction under continuous-flow conditions

…, R Heid, R Zhao, RS Rarig Jr, T Storz

文献索引：Tinder, Rob; Farr, Roger; Heid, Richard; Zhao, Ralph; Rarig Jr., Randy S.; Storz, Thomas Organic Process Research and Development, 2009 , vol. 13, # 6 p. 1401 - 1406

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被引用次数: 18

摘要

Azidoethyl phenyl sulfide, a readily accessible and reasonably stable synthon for ethyl azide with acceptable thermal safety properties, was investigated in a preliminary design space evaluation of a [3+ 2]-cycloaddition with cyanoacetamide under continuous-flow conditions in the Syrris AFRICA flow reactor.