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Online Monitoring of Microwave??Enhanced Reactions by UV/Vis Spectroscopy

E Heller, J Klöckner, W Lautenschläger…

文献索引:Heller, Eberhard; Kloeckner, Jessica; Lautenschlaeger, Werner; Holzgrabe, Ulrike European Journal of Organic Chemistry, 2010 , # 19 p. 3569 - 3573

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被引用次数: 8

摘要

Abstract Microwave-enhanced reactions are very fast in comparison to thermal reactions. They are often finished within a few minutes. Thus, the determination of the end point often fails, because conventional analytical methods are too slow. We developed a fast method using a UV/Vis sensor, which allows a direct online monitoring of the reaction process. The potency of the method is demonstrated by means of five representative reactions.