Tetrahedron letters

Selective and efficient synthesis of di-, tri-and tetrasubstituted 1, 10-phenanthrolines

C Dietrich-Buchecker, MC Jime, JP Sauvage

文献索引：Dietrich-Buchecker, Christiane; Jimenez, M. Consuelo; Sauvage, Jean-Pierre Tetrahedron Letters, 1999 , vol. 40, # 17 p. 3395 - 3396

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被引用次数: 44

摘要

A general synthetic procedure for the preparation of multisubstituted phenanthrolines is presented. Bromination of 1, 10-phenanthroline at the 3 and 8 positions, followed by Suzuki coupling reaction and subsequent methylation afford the di-, tri and tetra-substituted phenanthrolines in good yields. These phenanthroline derivatives are useful building blocks in the construction of highly sophisticated molecular architectures. 1, 10-Phenanthrolines1 ...