Facile Preparation and Purification of Mono tert??Butyl Malonate

VI Tararov, A Korostylev, G König…

文献索引：Tararov, Vitali I.; Korostylev, Andrei; Koenig, Gerd; Boerner, Armin Synthetic Communications, 2006 , vol. 36, # 2 p. 187 - 191

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被引用次数: 14

摘要

View all references Unfortunately, only lower monoesters or their salts are available at costs reasonable for preparative work, for example, EtO 2 CCH 2 CO 2 H, EtO 2 CCH 2 CO 2 K, and MeO 2 CCH 2 CO 2 K. In contrast the price of tert??BuO 2 CCH 2 CO 2 H, which is required for the simultaneous introduction of bulky tert??Bu protective group in the products, is extremely high. ... In our current work we were forced to find a simple and cheap method for ...