Tetrahedron letters

Synthesis of 1, 4-diazepin-5-ones under microwave irradiation and their reduction products

N Wlodarczyk, P Gilleron, R Millet, R Houssin…

文献索引：Wlodarczyk, Nicolas; Gilleron, Pauline; Millet, Regis; Houssin, Raymond; Henichart, Jean-Pierre Tetrahedron Letters, 2007 , vol. 48, # 14 p. 2583 - 2586

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被引用次数: 16

摘要

A new efficient access to 1, 4-diazepane derivatives is described via a microwave assisted synthesis of 7-substituted-1, 4-diazepin-5-ones, which proceeds rapidly in good yields. Catalytic reduction gave 1, 4-diazepan-5-ones and 1, 4-diazepanes whereas a ring ...