Synthesis of Novel Benzotriazoloazepine Derivatives

W Zhang, RB Han, WB Zhang…

文献索引：Zhang, Wei; Han, Rong-Bi; Zhang, Wen-Bin; Jiang, Ri-Shan; Piao, Feng-Yu Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 1 p. 29 - 32

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被引用次数: 1

摘要

Abstract Eight new benzotriazoloazepine derivatives have been synthesized starting from 7- methoxy-2, 3, 4, 5-tetrahydro-1H-2-benzo [c] azepin-1-one. The compounds 2a–c have been synthesized by the reaction of 7-methoxy-2, 3, 4, 5-tetrahydro-1H-2-benzo [c] azepin-1- thione with various hydrazides. Reaction of 5 with hydrazine hydrate, followed by treatment of the resultant hydrazone with formic acid, gave corresponding 9-alkoxy-6, 7-dihydro-5H- ...