Pentaerythritol derivatives. I. The preparation of pentaerythritol monomethyl ether1

CH Issidorides, AI Matar

文献索引：Issidorides; Matar Journal of the American Chemical Society, 1955 , vol. 77, p. 6382

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被引用次数: 14

摘要

Pentaerythrityl Monobromide (III).-The procedure of Beyaert and Hansensll was modified using 48% in place of 66% hydrobromic acid. Recrystallization of the final product from a mixture of 2 parts by volume of ethyl acetate and 3 parts by volume of chloroform gave monobromopentaerythritol (111) melting at 75-76'(reported mp 70-72", 11 76O12); yield 54% of the theoretical based on pentaerythritol.