... Volume: Page: Digital Object Identifier (DOI). ... (2 cc.) (if solid, a 1.5-g. portion was dissolved in the min. vol. MeOH), 10 cc. ... dild. with 50 cc. dry CCl4, refluxed 15 min., and worked up in the usual manner gave 18 g. III, b16 75-6°, nD20 1.4462. ...