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Sulfur nitride in organic chemistry. 6. Preparation of 3, 4??disubstituted 1, 2, 5??thiadiazoles by the reaction of sulfur nitride with acetylenes

S Mataka, K Takahashi, Y Yamada…

文献索引:Mataka,S. et al. Journal of Heterocyclic Chemistry, 1979 , vol. 16, p. 1009 - 1015

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被引用次数: 24

摘要

1010 S. Mataka, К. Takahashi, Y. Yamada, and M. Tashiro Vol. 16 the carboxylic acid (11) to give the known 3-phenyl-1,2,5- thiadiazole (3d) (6), which is a product of the reaction of 1 with 2d. И The structure 4b was confirmed as methyl 5-phenyl- l,2,4-thiadiazole-3-carboxylate by the treatment of 4b with concentrated ammonia to give the corresponding carbox- amide (12) (7). Compound 10 was determined to be methyl „Л 5-phenyl-l,2,3-thiadiazole-4- ...