The Journal of Organic Chemistry

Synthesis of alkyl trithioperesters (alkyl thiocarbonyl disulfides)

DF Aycock, GR Jurch Jr

文献索引：Aycock,D.F.; Jurch,G.R. Journal of Organic Chemistry, 1979 , vol. 44, # 4 p. 569 - 572

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被引用次数: 12

摘要

The first synthesis of alkyl trithioperesters (RC (S) SSR, alkyl thiocarbonyl disulfides) is described. t ert-Butyl trithiophenylperacetate (4) was synthesized starting with benzyl chloride. The Grignard of benzyl chloride is treated with carbon disulfide and hydrolyzed ...