Journal of the American Chemical Society

The Reaction of Arylamines with Diethyl Thionothiodiformate

R Sayre

文献索引：Sayre Journal of the American Chemical Society, 1952 , vol. 74, p. 3647

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被引用次数: 2

摘要

I/! I os nated as “thiodicarbomonothiodiarylamides. V'The reaction was carried out in each case at about 0'by adding the amine gradually to the ester dissolved in alcohol; the mixture was subsequently shaken with dilute hydrochloric acid in order to remove unreacted amine, and the solid product which separated at that point was filtered and crystallized from alcohol. In some instances Guha and Dutta added two moles of amine to one of ester, while in ...