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Journal of the American Chemical Society

CONDENSATIONS AND RING CLOSURES IN THE NAPHTHALENE SERIES. IV. A SYNTHESIS OF ACEPHENANTHRENE

LF Fieser, MA Peters

文献索引:Fieser; Peters Journal of the American Chemical Society, 1932 , vol. 54, p. 4373,4378

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被引用次数: 13

摘要

The possibility of preparing a still higher benzolog of acenaphthene by repeating the series of reactions used in the above syntheses was examined briefly. Condensed with succinic anhydride in nitrobenzene solution, tetrahydroacephenanthrene gave in good yield a keto acid which probably has the structure of X. This is inferred from the fact that sub-