The Journal of Organic Chemistry

Synthesis of L-threo-Pentulose and 3, 4, 5-Tri-O-benzoyl-1-deoxy-L-threo-pentulose1

ML Wolfrom, RB Bennett

文献索引：Wolfrom,M.L.; Bennett,R.B. Journal of Organic Chemistry, 1965 , vol. 30, p. 458 - 462

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被引用次数: 16

摘要

Deacetylation of the pentulose tetraacetate with barium hydroxide and preparative thin layer chromatography of the crude reaction product on microcrystalline cellulosez1 gave L-threo- pentulose (VII), characterized as the crystalline p-broniophenylhydra-L-threo-Pentulose showed a particular sensitivity to alkali as indicated by the formation, during the deacetylation process, of several products as detected by thin layer chromatography.