Vapor Phase Reactions of Styrene Chlorohydrin

WS Emerson, EP Agnew

文献索引：Emerson; Agnew Journal of the American Chemical Society, 1945 , vol. 67, p. 518,520

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被引用次数: 22

摘要

Method B: An alternative procedure was to add 0.33 inole of styrene chlorohydrin over a one- half hour period to a boiling mixture of 0.33 mole of the secondary amine and 50 cc. of water containing 42 g.(0.5 mole) of sodium bicarbonate. After refluxing seven hours, the mixture was cooled and extracted with benzene. Distillation of the benzene extract yielded the desired p-dialkylaniino-aphenylethyl alcohol.