Helvetica chimica acta

Effective Methods for the Synthesis of N??Methyl β??Amino Acids from All Twenty Common α??Amino Acids Using 1, 3??Oxazolidin??5??ones and 1, 3??Oxazinan??6??ones

AB Hughes, BE Sleebs

文献索引：Helvetica Chimica Acta, , vol. 89, # 11 p. 2611 - 2637

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被引用次数: 18

摘要

... Helvetica Chimica Acta – Vol. 89 (2006) 2622 ... The 1,3-oxazinan-6-one (1mmol) was dissolved in the minimum volume of CH2Cl2/ CF3CO2H 1:1 (v/v). Et3ACHTUNGTRENNUNGSiH (3 mmol) was added, and the mixture was stirred for 24–48 h, until no 1,3-oxazinan-6-one ...