Selective cleavage of N-benzyl-protected secondary amines by triphosgene

MG Banwell, MJ Coster, MJ Harvey…

文献索引：Journal of Organic Chemistry, , vol. 68, # 2 p. 613 - 616

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被引用次数: 26

摘要

... The Journal of Organic ... The combined organic portions were then dried (Na 2 SO 4 ), filtered, and concentrated under reduced pressure to give a yellow oil. ... compound 28 (1.01 g, 100%) as a clear, colorless oil: 1 H NMR (300 MHz) δ 7.40−7.20 (20H, m), 4.02 (2H, t, J = 6.3 Hz ...