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Tetrahedron

Total syntheses of prothracarcin and tomaymycin by use of palladium catalyzed carbonylation

M Mori, Y Uozumi, M Kimura, Y Ban

文献索引：Mori, Miwako; Uozumi, Yasuhiro; Kimura, Masaya; Ban, Yoshio Tetrahedron, 1986 ,  vol. 42,  # 14  p. 3793 - 3806

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被引用次数: 63

摘要

Tetrahedron Vol. 42, No. 14, pp. 3793 to 3806, 1986 W40-4020/86 H. OO+. OO Printed in Great Britain. Pcrgamon Journals Ltd. Total Syntheses of Prothracarcin and Tomaymycin by Use of Palladium Catalyzed Carbonylation Miwako Mori, Yasuhiro Uozumi, Masaya Kimura and Yoshio Ban Faculty of Pharmaceutical Sciences, Hokkaido University, Sapporo 060, Japan+ School of Pharmaceutical Sciences, Toho University, Miyama 2-2-1, Funabashi ...

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2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-56-2

2-iodo-N-methox...

~%

(R)-1-((2S,11aS)-2-hydroxy-10-(methoxymethyl)-5,11-dioxo-2,3,5,10,11,11a-hexahydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepin-2-yl)ethyl methanesulfonate结构式

108555-68-6

(R)-1-((2S,11aS...

2-iodo-N-(4-hydroxy-1-trifluoroacetyl-1-prolyl)aniline结构式

108555-53-9

2-iodo-N-(4-hyd...

~%

(R)-1-((2S,11aS)-2-hydroxy-10-(methoxymethyl)-5,11-dioxo-2,3,5,10,11,11a-hexahydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepin-2-yl)ethyl methanesulfonate结构式

108555-68-6

(R)-1-((2S,11aS...

2-iodo-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-54-0

2-iodo-N-(N-tri...

~%

(R)-1-((2S,11aS)-2-hydroxy-10-(methoxymethyl)-5,11-dioxo-2,3,5,10,11,11a-hexahydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepin-2-yl)ethyl methanesulfonate结构式

108555-68-6

(R)-1-((2S,11aS...

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-55-1

2-iodo-N-methox...

~%

(R)-1-((2S,11aS)-2-hydroxy-10-(methoxymethyl)-5,11-dioxo-2,3,5,10,11,11a-hexahydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepin-2-yl)ethyl methanesulfonate结构式

108555-68-6

(R)-1-((2S,11aS...

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-56-2

2-iodo-N-methox...

~%

(2S,11aS)-2-hydroxy-2-((R)-1-hydroxyethyl)-10-(methoxymethyl)-2,3-dihydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-5,11(10H,11aH)-dione结构式

108555-66-4

(2S,11aS)-2-hyd...

2-iodo-N-(4-hydroxy-1-trifluoroacetyl-1-prolyl)aniline结构式

108555-53-9

2-iodo-N-(4-hyd...

~%

(2S,11aS)-2-hydroxy-2-((R)-1-hydroxyethyl)-10-(methoxymethyl)-2,3-dihydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-5,11(10H,11aH)-dione结构式

108555-66-4

(2S,11aS)-2-hyd...

2-iodo-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-54-0

2-iodo-N-(N-tri...

~%

(2S,11aS)-2-hydroxy-2-((R)-1-hydroxyethyl)-10-(methoxymethyl)-2,3-dihydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-5,11(10H,11aH)-dione结构式

108555-66-4

(2S,11aS)-2-hyd...

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-56-2

2-iodo-N-methox...

~%

(11aS)(E)-2-ethylidene-2,3,5,10,11,11a-hexahydro-10-methoxymethyl-5,11-dioxo-1H-pyrrolo<2,1-c><1,4>benzodiazepine结构式

108555-65-3

(11aS)(E)-2-eth...

2-iodo-N-(4-hydroxy-1-trifluoroacetyl-1-prolyl)aniline结构式

108555-53-9

2-iodo-N-(4-hyd...

~%

(11aS)(E)-2-ethylidene-2,3,5,10,11,11a-hexahydro-10-methoxymethyl-5,11-dioxo-1H-pyrrolo<2,1-c><1,4>benzodiazepine结构式

108555-65-3

(11aS)(E)-2-eth...

2-iodo-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-54-0

2-iodo-N-(N-tri...

~%

(11aS)(E)-2-ethylidene-2,3,5,10,11,11a-hexahydro-10-methoxymethyl-5,11-dioxo-1H-pyrrolo<2,1-c><1,4>benzodiazepine结构式

108555-65-3

(11aS)(E)-2-eth...

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-55-1

2-iodo-N-methox...

~%

(11aS)(E)-2-ethylidene-2,3,5,10,11,11a-hexahydro-10-methoxymethyl-5,11-dioxo-1H-pyrrolo<2,1-c><1,4>benzodiazepine结构式

108555-65-3

(11aS)(E)-2-eth...

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-56-2

2-iodo-N-methox...

~%

(11aS)(Z)-2-ethylidene-2,3,5,10,11,11a-hexahydro-10-methoxymethyl-5,11-dioxo-1H-pyrrolo-<2,1-c><1,4>benzodiazepine结构式

108555-63-1

(11aS)(Z)-2-eth...

2-iodo-N-(4-hydroxy-1-trifluoroacetyl-1-prolyl)aniline结构式

108555-53-9

2-iodo-N-(4-hyd...

~%

(11aS)(Z)-2-ethylidene-2,3,5,10,11,11a-hexahydro-10-methoxymethyl-5,11-dioxo-1H-pyrrolo-<2,1-c><1,4>benzodiazepine结构式

108555-63-1

(11aS)(Z)-2-eth...

2-iodo-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-54-0

2-iodo-N-(N-tri...

~%

(11aS)(Z)-2-ethylidene-2,3,5,10,11,11a-hexahydro-10-methoxymethyl-5,11-dioxo-1H-pyrrolo-<2,1-c><1,4>benzodiazepine结构式

108555-63-1

(11aS)(Z)-2-eth...

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-55-1

2-iodo-N-methox...

~%

(11aS)(Z)-2-ethylidene-2,3,5,10,11,11a-hexahydro-10-methoxymethyl-5,11-dioxo-1H-pyrrolo-<2,1-c><1,4>benzodiazepine结构式

108555-63-1

(11aS)(Z)-2-eth...

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-56-2

2-iodo-N-methox...

~%

(11aS)-2,3,5,10,11,11a-Hexahydro-10-(methoxymethyl)-2,5,11-trioxo-1H-pyrrolo<2,1-c><1,4>benzodiazepine结构式

108555-61-9

(11aS)-2,3,5,10...

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-56-2

2-iodo-N-methox...

~%

(11aS)-2(R)-Hydroxy-2,3,5,10,11,11a-hexahydro-10-(methoxymethyl)-5,11-dioxo-1H-pyrrolo<2,1-c><1,4>benzodiazepine结构式

108555-60-8

(11aS)-2(R)-Hyd...

carbon monoxide结构式

201230-82-2

carbon monoxide

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-56-2

2-iodo-N-methox...

~93%

(2R,11aS)-2-(methoxymethoxy)-10-(methoxymethyl)-2,3-dihydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-5,11(10H,11aH)-dione结构式

108555-58-4

(2R,11aS)-2-(me...

2-iodo-N-(4-hydroxy-1-trifluoroacetyl-1-prolyl)aniline结构式

108555-53-9

2-iodo-N-(4-hyd...

~%

(2R,11aS)-2-(methoxymethoxy)-10-(methoxymethyl)-2,3-dihydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-5,11(10H,11aH)-dione结构式

108555-58-4

(2R,11aS)-2-(me...

2-iodo-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-54-0

2-iodo-N-(N-tri...

~%

(2R,11aS)-2-(methoxymethoxy)-10-(methoxymethyl)-2,3-dihydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-5,11(10H,11aH)-dione结构式

108555-58-4

(2R,11aS)-2-(me...

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-55-1

2-iodo-N-methox...

~90%

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-56-2

2-iodo-N-methox...

2-iodo-N-(4-hydroxy-1-trifluoroacetyl-1-prolyl)aniline结构式

108555-53-9

2-iodo-N-(4-hyd...

~%

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-56-2

2-iodo-N-methox...

2-iodo-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-54-0

2-iodo-N-(N-tri...

~%

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-56-2

2-iodo-N-methox...

2-iodo-N-(4-hydroxy-1-trifluoroacetyl-1-prolyl)aniline结构式

108555-53-9

2-iodo-N-(4-hyd...

~%

2-iodo-N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)aniline结构式

108555-55-1

2-iodo-N-methox...


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