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Synthesis, characterization and biological activities of some new organotin (IV) derivatives: Crystal structure of [(Sn Ph 3)(OOCC 6 H 4 OH)] and [(SnMe 3) 2 (OOC) 2 …

MK Rauf, MA Saeed, M Bolte, A Badshah…

文献索引:Khawar Rauf; Adeel Saeed; Imtiaz-ud-Din; Bolte; Badshah; Mirza Journal of Organometallic Chemistry, 2008 , vol. 693, # 18 p. 3043 - 3048

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被引用次数: 41

摘要

Some new organotin (IV) carboxylates 1–3 of 2-hydroxybenzoic acid (LA) and 4–6 of 2, 3, 4, 5-tetrachloro-6-(methoxycarbonyl) benzoic acid (LB) have been synthesized, respectively, by the esterification of triorganotin oxide/hydroxide with the corresponding acids in an appropriate mole ratios. Multinuclear NMR (1H, 13C and 119Sn), IR and X-ray crystallographic studies were carried out to elucidate their structures both in solution and ...