Heterocyclic Vinyl Ethers. XII. The Synthesis of Arylmercaptoacetylenes and a New Cleavage Reaction of Benzo-1, 4-dithiadiene1, 2

WE Parham, PL Stright

文献索引：Parham; Stright Journal of the American Chemical Society, 1956 , vol. 78, p. 4783,4785

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被引用次数: 35

摘要

I SI11 i SIT bility we repeated the reaction using excess n-butyllithium and one equivalent of dimethyl sulfate.-1 vigorous reaction occurred, and the neutral product (46Yc yield), thus obtained, was subsequently identified as the hitherto unknown 1-(n-butylthio)-2- methylthiobenzene (XIII). This product was characterized by conversion to sulfone XI\'and the sulfonyl chlo-The structures of XIII. XIV and XV were established by their independent ...